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Discovery of AZD3839, a potent and selective BACE1 inhibitor clinical candidate for the treatment of Alzheimer disease

Bibliographic

Year of Publication:
2012
Contact PI Name:
Johanna Falting
Contact PI Affiliation:
AstraZeneca Research and Development, Innovative Medicines, CNS and Pain, Sodertalje, Sweden
Co-Authors:
Fredrik Jeppsson, Susanna Eketjall, Juliette Janson, Sofia Karlstrom, Susanne Gustavsson, Lise-Lotte Olsson, Ann-Cathrine Radesater, Bart Ploeger, Gvido Cebers, Karin Kolmodin, Britt-Marie Swahn, Stefan von Berg, Tjerk Bueters
Primary Reference (PubMED ID):
Funding Source:
AstraZeneca Research and Development Innovative Medicines CNS and Pain Sweden
Study Goal and Principal Findings:

β-Site amyloid precursor protein cleaving enzyme1 (BACE1) is one of the key enzymes involved in the processing of the amyloid precursor protein (APP) and formation of amyloid β peptide (Aβ) species. Because cerebral deposition of Aβ species might be critical for the pathogenesis of Alzheimer disease, BACE1 has emerged as a key target for the treatment of this disease. Here, we report the discovery and comprehensive preclinical characterization of AZD3839, a potent and selective inhibitor of human BACE1. AZD3839 was identified using fragment-based screening and structure-based design. In a concentration-dependent manner, AZD3839 inhibited BACE1 activity in a biochemical fluorescence resonance energy transfer (FRET) assay, Aβ and sAPPβ release from modified and wild-type human SH-SY5Y cells and mouse N2A cells as well as from mouse and guinea pig primary cortical neurons. Selectivity against BACE2 and cathepsin D was 14 and >1000-fold, respectively. AZD3839 exhibited dose- and time-dependent lowering of plasma, brain, and cerebrospinal fluid Aβ levels in mouse, guinea pig, and non-human primate. Pharmacokinetic/pharmacodynamic analyses of mouse and guinea pig data showed a good correlation between the potency of AZD3839 in primary cortical neurons and in vivo brain effects. These results suggest that AZD3839 effectively reduces the levels of Aβ in brain, CSF, and plasma in several preclinical species. It might, therefore, have disease-modifying potential in the treatment of Alzheimer disease and related dementias. Based on the overall pharmacological profile and its drug like properties, AZD3839 has been progressed into Phase 1 clinical trials in man.

Therapeutic Agent

Therapeutic Information:
Therapy Type:
Small Molecule
Therapeutic Agent:
AZD3839
Therapeutic Target:
BACE1

Animal Model

Model Information:
Species:
Mouse
Model Type:
Non-transgenic
Strain/Genetic Background:
C57BL/6
Species:
Guinea Pig
Model Type:
Outbred
Strain/Genetic Background:
Not Applicable
Species:
Non Human Primate
Model Type:
Non-transgenic
Strain/Genetic Background:
Not Applicable

Experimental Design

Is the following information reported in the study?:
Power/Sample Size Calculation
Randomized into Groups
Blinded for Treatment
Blinded for Outcome Measures
Pharmacokinetic Measures
Pharmacodynamic Measures
Toxicology Measures
ADME Measures
Biomarkers
Dose
Formulation
Route of Delivery
Duration of Treatment
Frequency of Administration
Age of Animal at the Beginning of Treatment
Age of Animal at the End of Treatment
Sex as a Biological Variable
Study Balanced for Sex as a Biological Variable
Number of Premature Deaths
Number of Excluded Animals
Statistical Plan
Genetic Background
Inclusion/Exclusion Criteria Included
Conflict of Interest

Outcomes

Outcome Measured
Outcome Parameters
Biochemical
Brain-beta Amyloid Peptide 40
Brain-beta Amyloid Peptide 42
Soluble Amyloid Precursor Protein beta (sAPP beta)
beta-Site Amyloid Precursor Protein Cleaving Enzyme 2 (BACE2)
Cathepsin D
Emax
IC50
Spectroscopy
Liquid Chromatography with Tandem Mass Spectrometry (LC/MS/MS)
Cell Biology
Cell Viability
Cytotoxicity
Soluble Amyloid Precursor Protein beta (sAPP beta) Secretion
beta Amyloid Peptide Secretion
Biomarker
CSF-beta Amyloid Peptide 40
CSF-beta Amyloid Peptide 42
CSF-Soluble Amyloid Precursor Protein beta (sAPP beta)
Plasma-beta Amyloid Peptide 40
Plasma-beta Amyloid Peptide 42
Pharmacokinetics
Brain/Plasma Ratio
Brain/CSF Ratio
CSF/Plasma Ratio
Drug Concentration-Brain
Drug Concentration-CSF
Drug Concentration-Plasma
Free Drug Concentration-Brain
Free Drug Concentration-CSF
Free Drug Concentration-Plasma
PK/PD Modeling
Pharmacodynamics
Target Engagement (Reduction beta Amyloid Peptide 40-Brain)
Target Engagement (Reduction beta Amyloid Peptide 42-Brain)
Target Engagement (Reduction Soluble Amyloid Precursor Protein beta)
ADME
Plasma Protein Binding
Brain Tissue Binding
Pharmacology
Target Selectivity